Aim :- Grey water Parameter Testing

Objective :- Check the TDS,ph,salt,EC and COD of Graywater sample for the application of greywater reuse in urban water systems provides substantial benefits for both the water supply subsystem by reducing the demand for fresh clean water

Introduction :-

Greywater (also spelled graywater, grey waterand gray water) or sullage is all wastewatergenerated in households or office buildings from streams without fecal contamination, i.e. all streams except for the wastewater from toilets. Sources of greywater include, sinks, showers, baths, clothes washing machines or dish washers. As greywater contains fewer pathogens than domestic wastewater, it is generally safer to handle and easier to treat and reuse onsite for toilet flushing, landscape or crop irrigation, and other non-potable uses.
The application of greywater reuse in urban water systems provides substantial benefits for both the water supply subsystem by reducing the demand for fresh clean water as well as the wastewater subsystems by reducing the amount of wastewater required to be conveyed and treated.Treated greywater has many uses, for example toilet flushing or irrigation.

Types of water:-

  1. Grey water :- Greywater can be Defined as any domestic wastewater produced , excluding sewage . The Main difference between Greywater and sewage is the organic loading . sewage has a much larger organic loading compared to greywater.
  2. Black water :- Blackwater is the mixture of urine, feces and flushwater along with anal cleansing water (if water is used for cleansing) and/or dry cleansing materials. … Water coming from domestic equipment other than toilets (e.g., bathtubs, showers, sinks, washing machines) is called greywater.
  3. Surface water :- Surface water is water on the surface of continents such as in a river, lake, or wetland. It can be contrasted with groundwater and atmospheric water. Non-saline surface water uses is replenished by precipitation and by recruitment from ground-water.
  4. Ground water :- Groundwater is the water present beneath Earth’s surface in soil pore spaces and in the fractures of rock formations. A unit of rock or an unconsolidated deposit is called an aquifer when it can yield a usable quantity of water.

Appratus :-

  1. Digester
  2. C.O.D. Tube
  3. Beaker
  4. Condenser
  5. Conical flask
  6. Burate Stand
  7. Funnel
  8. T.D.S. Meter

Parameter:– A numerical or other measurable factor forming one of a set that defines a system of sets the conditions of its operation

  1. TDS(Total dissolved solids):- Total amount of change ion including mineral, sulphate, water metal is called as TDS.
  2. Ph(potential of hydrogen):- It is a measure of hydrogen ion concentration a measure of the acidity or alkalinity of a solution is called as ph.
  3. EC(Electrical conductivity ) :- It is the fundamental property of a material that confitised how strongly it resists for the flow of electrical conductivity.
  4. Salt:- It is mineral compose primarily of sodium chloride (NaCl ).
  5. DO (dissolved oxygen):- Level of free oxygen present in water
  6. COD (Chemical oxygen demand):- It is a measure of the capacity of water to oxygen during the decomposition of organic matter
Measuring TDS

Date :- 04 – 06 – 2019

Sample reading :-

Water sampleSalt
(PPM)
PH

TDS
(ppm)
EC
(μs)
Basin water
kitchen
314
(ppm)
7.85

421
(ppm)
594 (μs)
Dream house312
(ppm)
7.78

432
(ppm)
613 (μs)
Food lab318
(ppm)
8.96

427
(ppm)
602 (μs)
Microbiology lab342
(ppm)
8.76

461
(ppm)
651 (μs)
Boys hostel257
(ppm)
7.85

349
(ppm)
491 (μs)

Conclusion :- 1. The sample which was taken from microbiology lab has more salt , TDS & EC

2. It was Found That Food lab sample has more PH

Date :- 09 – 06 – 2019

Reading Sample :-

water sampleSalt
(ppm)
PH

TDS
(ppm)
EC
(μs)
DO
(ppm)
Kitchen Basin314
(ppm)
10

429
(ppm)
595 (μs)0.65
(ppm)
Dream house301
(ppm)
9.8

407
(ppm)
571 (μs)5.28
(ppm)
Microbiology Lab290
(ppm)
9.39

389
(ppm)
551 (μs)3.99
(ppm)
Boys hostel Inlet153
(ppm)
9.6

140
(ppm)
197 (μs)0.80
(ppm)

Conclusion :- It Was Found that kitchen basin water has highest salt , PH , TDS & EC.

DO Calibration

Date :- 12 – 06 – 2019

Sample Readings :-

Water SampleSalt
(ppm)
PH

TDS
(ppm)
EC
(μs)
Microbiology lab219
(ppm)
10.34

296
(ppm)
420 (μs)
Dream House290
(ppm)
10.93

392
(ppm)
554 (μs)
Boys Hostel292
(ppm)
10.44

394
(ppm)
555 (μs)
Kitchen Basin356
(ppm)
10.69

474
(ppm)
672 (μs)
Girls Hostel Inlet1.51
(ppm)
10.96

1.91
(ppm)
2.66 (μs)
Kitchen Inlet Grey water502
(ppm)
10.28

667
(ppm)
938 (μs)
Grey water outlet485
(ppm)
10.43

646
(ppm)
907 (μs)

Conclusion :- Kitchen Inlet Greywater has more amount of salt , TDS & EC.

It was found that PH of Dream house Is more than any other sample.

Date :- 14 – 6 – 2019

Sample Reading :-

SamplePH

EC
(μs)
TDS
(ppm)
Salt
(ppm)
Boys Hostel8.12

1730 (μs)1.23
(ppm)
956
(ppm)
Grey Water Inlet7.94

1194 (μs)853
(ppm)
645
(ppm)
Grey Water Outlet7.85

1305 (μs)925
(ppm)
705
(ppm)

Conclusion :- 1. Boys Hostel sample has more PH , EC & salt

2. TDS Of Grey water outlet Found more

Date :- 17 – 06 – 2019

Sample Reading :-

SamplePH

Salt
(ppm)
EC
(μs)
TDS
(ppm)
Greywater Inlet7.22

509
(ppm)
944 (μs)664
(ppm)
Greywater Outlet7.35

560
(ppm)
1052 (μs)740
(ppm)

Conclusion :- Greywater Outlet has more PH , Salt , EC & TDS

Procedure of DO ( Dissolved oxygen) :-

  1. Connect the DO probe and temp. probe to meter and remove the protection cap from the probe
  2. Remove the membrane cap carefully
  3. Fill the membrane cap with the electrolyte solution up to the bottom of the threads on the inside of the cap .

C.O.D. (Chemical oxygen demand ) :- Indicative Measure of the amount of oxygen that can be consumed by ractions in a measured solution quantity the amount of organics in water

Quantity amount of oxidizable pollutants found in surface water/wastewater.

Adition table :-

Samplek2cr2o7Distilled waterH2SO4
Inlet510ml35ml30ml
outlet510ml35ml30ml
KHP2010ml20ml30ml
Blank10ml40ml30ml

C.O.D. Procedure :-

  1. Take 0.4 HgSo4 (mercuric Surface) in COD Tube
  2. Add 10ml ( 0.25N) K2Cr2O7 Solution ( Dicromate Solution)
  3. Add Stone ( Cruston Beads )
  4. Add 30ml Can Sulfuric Acid Slowly Along With swirling
  5. If turn green , Add more Quantity Of K2Cr2O7
  6. Mix , Attach Condensor
  7. Keep at 150℃ For 2 hrs. then cool , wash condensor with D.W.
  8. Add About 150 D.W.
  9. Titrate With 0.1 N FAS ( Terrous Ammonium Bulfite )

Blue green – Reddish Brown

Date :- 12 – 06 -2019

Kitchen Water –

  1. Blank – 14.5
  2. KHP – 23
  3. Inlet – 33.8
  4. Outlet – 45
  • KHP – 23 – 14.5 = 8.5
  • Inlet – 33.8 – 23 = 10.8
  • Outlet – 45 – 33.8 = 11.2

C.O.D. = Blank -( Sample Reading) × 0.255 × 8000 ÷ 20

KHP = (14.5 – 8.5 ) × 0.255 × 8000 ÷ 20

= 612

Inlet = ( 14.5 – 10.8) × 0.255 × 8000 ÷ 20

= 377.4 × 4

= 1509.6

Outlet = ( 14.5 – 11.2) × 0.255 × 8000 ÷ 20

= 336.6 × 4

= 1346.4

Date :- 17 – 06 – 2019

Grey water :-

  1. Blank – 13.9
  2. KHP – 22.6
  3. Inlet – 31.3
  4. outlet – 44.3
  • KHP- 22.6 – 13.9 = 8.7
  • Inlet – 31.3- 22.6= 8.7
  • Outlet – 44.3 – 31.3=13

KHP = (13.9 – 8.7) × 0.255 × 8000 ÷ 20

= 530.4

Inlet = (13.9 – 8.7) × 0.255 × 8000 ÷ 20

= 830.4 × 4

= 2121.6

Outlet = (13.9 – 13) × 0.255 × 8000 ÷ 20

= 91.8 × 4

= 367.2

Date :- 21 – 06 – 2019

Sample Reading :-

Sample PHEC
(μs)
Salt
(ppm)
TDS
(ppm)
Kitchen Inlet7.958.91
(μs)
472
(ppm)
625
(ppm)
Kitchen Outlet7.8110.31
(μs)
553
(ppm)
729
(ppm)

Date :- 24 – 06 – 2019

Sample Reading :-

SampleTDS
(ppm)
PH

Salt
(ppm)
EC
(μs)
Grey water Inlet616
(ppm)
8.03

457
(ppm)
865
(μs)
Grey water Outlet769
(ppm)
8.12535
(ppm)
1082
(μs)

Date :- 24 – 06 – 2019

COD :-

  1. Blank – 13.5
  2. KHP – 21.9
  3. Inlet – 31.3
  4. Outlet – 43.8
  • KHP – 21.9 – 13.5 = 8.4
  • Inlet – 31.3 – 21.9 = 9.4
  • Outlet – 43.8 – 31.8 = 12

COD = Blank – ( Sample Reading × 0.255 × 8000 ÷ 20

KHP = (13.5 – 8.4 ) × 0.255 × 8000 ÷ 20=520.2

= 520.2 ×4

= 2080.8

Inlet = (13.5 – 9.4 ) × 0.255 × 8000 ÷ 20=418.2

= 418.2×4

= 1622.8

Outlet = ( 13.5 – 12 ) × 0.255 × 8000 ÷ 20=153

= 153 × 4

= 612

Date :- 27 – 06 – 2019

Sample Reading :-

SampleTDS
(ppm)
salt
(ppm)
PHEC
(μs)
Kitchen Inlet685
(ppm)
509
(ppm)
8.37960
(μs)
Kitchen Outlet608
(ppm)
455
(ppm)
8.45853
(μs)

Date :- 27 – 06 – 2019

COD :-

  1. Blank – 24
  2. KHP – 45 & 2.5 =45 + 2.5 = 47.5
  3. Inlet – 36
  4. Outlet – 18
  • KHP = 47.5 – 24 = 23.5
  • Inlet = 36 – 47.5 = -11.5
  • Outlet = 18 – 36 = -18

COD = Blank – ( Sample Reading × 0.255 × 8000 ÷ 20

KHP = 24 – 23.5 × 0.255 × 8000 ÷ 20

= 51 × 4

= 204

Inlet = 24 – ( -11.5 ) × 0.255 × 8000 ÷ 20

= 3621 × 4

= 14,484

Outlet = 24 – ( -18) × 0.255 × 8000 ÷ 20

= 4284 × 4

= 17,136